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Atomic
Force Microscopy adds a whole new dimension to your laboratory
capability. AFM gives you more than SEM's 2-D images of a surface -
AFM provides true 3-D topographic images which also yield surface
roughness data on the nano-meter scale. Consequently, AFM is ideal
for characterizing metal coatings and finished surfaces, and can
provide surface roughness data that is similar to that of a
profilometer. In addition to providing topographic data, AFM can
also reveal information such as the relative frictional properties
of heterogeneous phases.
The two images of a Zn
electrode below illustrate the large range of areas and
resolutions that can be examined with AFM, from tens of microns to
the nanometer scale.


When
a typical commercial razor blade is used for cutting, a teflon
coating on the stainless steel blade continually erodes until a thin
residual layer is all that remains. The continuity of this layer is
difficult to resolve from the steel in topography images, and is
almost impossible to image otherwise; yet, with the use of lateral
force mode, the frictional behavior of the teflon stands out
strongly from the metallic substrate, revealing the degree of
dispersion of the teflon. In this case, brighter metallic regions
are "stickier" than the teflon in Lateral Force Mode. This
is intuitively correct, since teflon is often called a
"non-stick" material.

The
AFM topography images below were taken from corroded sheet metal.
The image at left was taken outside the corrosion halo and shows a
polishing texture that is typical of finished metals. The corrosion
halo at right has a strikingly different surface texture relative to
the virgin surface, yet its surface roughness does not differ from
the polishing texture. An SEM analysis reveals little in this study
because it cannot adequately resolve these surface textures in the
z-direction, and neither can SEM give us meaningful z-roughness
data.

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